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Characterization and analyte selectivity of Ag-Cu NPs. (a) Optical images and UV-Vis spectra of Ag-Cu NPs before (colorless) and after (yellow colloid) heat treatment; (b) TEM image of Ag-Cu NPs (inset: magnified view of selected area); (c) EDX elemental maps and HAADF-STEM image of Ag-Cu NPs; (d) FTIR spectra of Ag-Cu NPs; (e-f) Selectivity of Ag-Cu NPs toward (e) VOCs and (f) ions. UV-Vis spectra of Ag-Cu NPs synthesized under different conditions: (g) Effect of d -mannitol concentration (0.05, 0.1, 0.2, and 0.4 mg/mL) with fixed AgNO₃ (1 mM), CuSO₄ (0.1 mM), and TSC (0.25 mM); (h) Effect of TSC concentration (0, 0.25, 0.5, and 1 mM) with fixed d -mannitol (0.1 mg/mL), AgNO₃ (1 mM), and CuSO₄ (0.1 mM); (i) Effect of Ag/Cu molar ratios (I-0.1: AgNO₃ 1 mM/CuSO₄ 0.1 mM; I-0.5: 1 mM/0.5 mM; I-1: 1 mM/1 mM; I-2: 1 mM/2 mM) with fixed d -mannitol (0.1 mg/mL) and TSC (0.25 mM).
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Characterization and analyte selectivity of Ag-Cu NPs. (a) Optical images and UV-Vis spectra of Ag-Cu NPs before (colorless) and after (yellow colloid) heat treatment; (b) TEM image of Ag-Cu NPs (inset: magnified view of selected area); (c) EDX elemental maps and HAADF-STEM image of Ag-Cu NPs; (d) FTIR spectra of Ag-Cu NPs; (e-f) Selectivity of Ag-Cu NPs toward (e) VOCs and (f) ions. UV-Vis spectra of Ag-Cu NPs synthesized under different conditions: (g) Effect of d -mannitol concentration (0.05, 0.1, 0.2, and 0.4 mg/mL) with fixed AgNO₃ (1 mM), CuSO₄ (0.1 mM), and TSC (0.25 mM); (h) Effect of TSC concentration (0, 0.25, 0.5, and 1 mM) with fixed d -mannitol (0.1 mg/mL), AgNO₃ (1 mM), and CuSO₄ (0.1 mM); (i) Effect of Ag/Cu molar ratios (I-0.1: AgNO₃ 1 mM/CuSO₄ 0.1 mM; I-0.5: 1 mM/0.5 mM; I-1: 1 mM/1 mM; I-2: 1 mM/2 mM) with fixed d -mannitol (0.1 mg/mL) and TSC (0.25 mM).
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Characterization and analyte selectivity of Ag-Cu NPs. (a) Optical images and UV-Vis spectra of Ag-Cu NPs before (colorless) and after (yellow colloid) heat treatment; (b) TEM image of Ag-Cu NPs (inset: magnified view of selected area); (c) EDX elemental maps and HAADF-STEM image of Ag-Cu NPs; (d) FTIR spectra of Ag-Cu NPs; (e-f) Selectivity of Ag-Cu NPs toward (e) VOCs and (f) ions. UV-Vis spectra of Ag-Cu NPs synthesized under different conditions: (g) Effect of d -mannitol concentration (0.05, 0.1, 0.2, and 0.4 mg/mL) with fixed AgNO₃ (1 mM), CuSO₄ (0.1 mM), and TSC (0.25 mM); (h) Effect of TSC concentration (0, 0.25, 0.5, and 1 mM) with fixed d -mannitol (0.1 mg/mL), AgNO₃ (1 mM), and CuSO₄ (0.1 mM); (i) Effect of Ag/Cu molar ratios (I-0.1: AgNO₃ 1 mM/CuSO₄ 0.1 mM; I-0.5: 1 mM/0.5 mM; I-1: 1 mM/1 mM; I-2: 1 mM/2 mM) with fixed d -mannitol (0.1 mg/mL) and TSC (0.25 mM).
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d mannitol  (Fisher Scientific)
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Fisher Scientific d mannitol
Characterization and analyte selectivity of Ag-Cu NPs. (a) Optical images and UV-Vis spectra of Ag-Cu NPs before (colorless) and after (yellow colloid) heat treatment; (b) TEM image of Ag-Cu NPs (inset: magnified view of selected area); (c) EDX elemental maps and HAADF-STEM image of Ag-Cu NPs; (d) FTIR spectra of Ag-Cu NPs; (e-f) Selectivity of Ag-Cu NPs toward (e) VOCs and (f) ions. UV-Vis spectra of Ag-Cu NPs synthesized under different conditions: (g) Effect of d -mannitol concentration (0.05, 0.1, 0.2, and 0.4 mg/mL) with fixed AgNO₃ (1 mM), CuSO₄ (0.1 mM), and TSC (0.25 mM); (h) Effect of TSC concentration (0, 0.25, 0.5, and 1 mM) with fixed d -mannitol (0.1 mg/mL), AgNO₃ (1 mM), and CuSO₄ (0.1 mM); (i) Effect of Ag/Cu molar ratios (I-0.1: AgNO₃ 1 mM/CuSO₄ 0.1 mM; I-0.5: 1 mM/0.5 mM; I-1: 1 mM/1 mM; I-2: 1 mM/2 mM) with fixed d -mannitol (0.1 mg/mL) and TSC (0.25 mM).
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Characterization and analyte selectivity of Ag-Cu NPs. (a) Optical images and UV-Vis spectra of Ag-Cu NPs before (colorless) and after (yellow colloid) heat treatment; (b) TEM image of Ag-Cu NPs (inset: magnified view of selected area); (c) EDX elemental maps and HAADF-STEM image of Ag-Cu NPs; (d) FTIR spectra of Ag-Cu NPs; (e-f) Selectivity of Ag-Cu NPs toward (e) VOCs and (f) ions. UV-Vis spectra of Ag-Cu NPs synthesized under different conditions: (g) Effect of d -mannitol concentration (0.05, 0.1, 0.2, and 0.4 mg/mL) with fixed AgNO₃ (1 mM), CuSO₄ (0.1 mM), and TSC (0.25 mM); (h) Effect of TSC concentration (0, 0.25, 0.5, and 1 mM) with fixed d -mannitol (0.1 mg/mL), AgNO₃ (1 mM), and CuSO₄ (0.1 mM); (i) Effect of Ag/Cu molar ratios (I-0.1: AgNO₃ 1 mM/CuSO₄ 0.1 mM; I-0.5: 1 mM/0.5 mM; I-1: 1 mM/1 mM; I-2: 1 mM/2 mM) with fixed d -mannitol (0.1 mg/mL) and TSC (0.25 mM).

Journal: Poultry Science

Article Title: Eco-friendly synthesis of Ag-Cu NPs via mannitol reduction for meat freshness monitoring

doi: 10.1016/j.psj.2025.106355

Figure Lengend Snippet: Characterization and analyte selectivity of Ag-Cu NPs. (a) Optical images and UV-Vis spectra of Ag-Cu NPs before (colorless) and after (yellow colloid) heat treatment; (b) TEM image of Ag-Cu NPs (inset: magnified view of selected area); (c) EDX elemental maps and HAADF-STEM image of Ag-Cu NPs; (d) FTIR spectra of Ag-Cu NPs; (e-f) Selectivity of Ag-Cu NPs toward (e) VOCs and (f) ions. UV-Vis spectra of Ag-Cu NPs synthesized under different conditions: (g) Effect of d -mannitol concentration (0.05, 0.1, 0.2, and 0.4 mg/mL) with fixed AgNO₃ (1 mM), CuSO₄ (0.1 mM), and TSC (0.25 mM); (h) Effect of TSC concentration (0, 0.25, 0.5, and 1 mM) with fixed d -mannitol (0.1 mg/mL), AgNO₃ (1 mM), and CuSO₄ (0.1 mM); (i) Effect of Ag/Cu molar ratios (I-0.1: AgNO₃ 1 mM/CuSO₄ 0.1 mM; I-0.5: 1 mM/0.5 mM; I-1: 1 mM/1 mM; I-2: 1 mM/2 mM) with fixed d -mannitol (0.1 mg/mL) and TSC (0.25 mM).

Article Snippet: D-Mannitol (>98%), silver nitrate (AgNO 3 , ≥99.8%), CuSO 4 , 99%, trisodium citrate (TSC, >99.5%), agar (BR), sodium sulfide nonahydrate (Na 2 S·9H 2 O, >98%), all chemical reagents, including flavor substances and various ions, were obtained from Shanghai Yuanye Bio Technology Co., Ltd. Meat samples (pork and whiteleg shrimp) were purchased from Freshippo (Hema).

Techniques: Synthesized, Concentration Assay